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Beilstein J. Org. Chem. 2007, 3, No. 7, doi:10.1186/1860-5397-3-7
Graphical Abstract
Scheme 1: Electrochemical generation of carbocations by oxidative C-C bond dissociation.
Scheme 2: Electrochemical generation and accumulation of organosilicon cation by oxidative Si-Si bond dissoci...
Figure 1: Oxidation potentials (Ed; decomposition potential) of disilanes determined by rotating disk electro...
Figure 2: Optimized structures of radical cations of 1,2-diphenyldisilane and 1,2-bis [o-(2-pyridyl)- phenyl]...
Scheme 3: Electrochemical generation of organosilicon cation 3d.
Figure 3: CSI-MS of organosilicon cation 3d at 0°C.
Figure 4: Optimized structures of organosilicon cation 3d and silyl radical 4d by DFT calculations (B3LYP/LAN...
Scheme 4: Reaction of organosilicon cation 3d with p-tolylmagnesium bromide.